Dichloromethane → HCID 136364222, compound

Participants

Reaction Steps

To a solution of Zn-3 (82 mg, 93.2 μmol) in THF (9 mL) was added a suspension of K2CO3 (30 mg, 217 μmol) in methanol (3 mL). The mixture was stirred for 1 h at room temperature in the dark. Then CH2Cl2 (20 mL) was added. The mixture was washed with aqueous 5% NaHCO3 solution (20 niL) and dried (Na2SO4). Purification by column chromatography (silica, CH2Cl2/hexanes 1:2) afforded 58 mg (71.6 μmol, 77%) of the title compound as a red-purple solid.

Provenance & Evidence