Potassium Hydroxide → 4-Hydroxy-1-(2-hydroxycyclohexyloxy)-2,2,6,6-tetramethylpiperidine

HRID 650434Notes

Reaction equation

HRID 650434 reaction equation

C([O:9][CH:10]1[CH2:15][C:14]([CH3:17])([CH3:16])[N:13]([O:18][CH:19]2[CH2:24][CH2:23][CH2:22][CH2:21][CH:20]2[OH:25])[C:12]([CH3:27])([CH3:26])[CH2:11]1)(=O)C1C=CC=CC=1.[OH-].[K+]>CO>[OH:9][CH:10]1[CH2:15][C:14]([CH3:17])([CH3:16])[N:13]([O:18][CH:19]2[CH2:24][CH2:23][CH2:22][CH2:21][CH:20]2[OH:25])[C:12]([CH3:27])([CH3:26])[CH2:11]1

Participants

4

Reactant 2

HCID 14797Potassium Hydroxide

HCID 225076454-Benzoyloxy-1-(2-hydroxycyclohexyloxy)-2,2,6,6-tetramethylpiperidine

Product 1

HCID 225076354-Hydroxy-1-(2-hydroxycyclohexyloxy)-2,2,6,6-tetramethylpiperidine

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound is prepared by heating the compound prepared in Example 34 in a solution of potassium hydroxide in methanol.

Sources & evidence

ORD record: ord-68231a4a73964f2c8d6379c0d6600e0d
Source dataset: uspto-grants-2001_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06271377B1

Reaction notes

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