HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 21709913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 21709907 | HCID 21709907 | — |
| Product | HCID 21709913 | HCID 21709913 | — |
Reaction Steps
Similarly to the method described in intermediate 1.2, 22.8 g (0.23 mol) of phosgene, 10 g (76 mmol) of methyl(tetrahydro-2H-thiopyran-4-yl)amine and 7.8 g (76 mmol) of triethylamine were reacted. Yield 13.4 g. MS (m/z): 193 [M]+, 158 [M−Cl]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277790B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-0fa8132e9eaf49ad8b8d104a8bd6f460 |
| Source note | uspto-grants-2001_08 |