HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HC Yellow no. 13
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 4-Chloro-alpha,alpha,alpha-trifluoro-3-nitrotoluene | HCID 8462 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HC Yellow no. 13 | HCID 2799157 | — |
Reaction Steps
112.8 g (0.5 mol) of 4-chloro-3-nitrobenzotrifluoride and 61.1 g (1 mol) of 2-ethanolamine were heated in 50 ml of dimethylformamide at 100° C. for 2 h. The reaction mixture was then concentrated under reduced pressure, and water was added to the residue. The precipitate was filtered off with suction and recrystallized from cyclohexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277850B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-c2e51fcf758e4e8393ec6a1b60ac460c |
| Source note | uspto-grants-2001_08 |