HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22597833, compound → HCID 22597863, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22597833 | HCID 22597833 | — |
| Reactant | HCID 178418546 | HCID 178418546 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 22597863 | HCID 22597863 | — |
Reaction Steps
Ethyl 2-ethoxy-4-iso-propyl-5-bromobenzoate (1.2 g, 3-8 mmol) was treated with copper (I) cyanide (682 mg, 7.6 m.mol) in N-methyl-2-pyrrolidinone (40 ml) as described in Procedure 5 to give the title compound as an oil (400 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277861B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-bcbb566a12be4d7abf199b02ca27668b |
| Source note | uspto-grants-2001_08 |