2-Bromo-1-(3-nitrophenyl)ethan-1-one → HCID 21710899, compound

HRID 651026Notes

Reaction equation

HRID 651026 reaction equation
[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[C:4]([NH:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH:3]=1.Br[CH2:17][C:18]([C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([N+:26]([O-:28])=[O:27])[CH:21]=1)=O>>[NH2:7][C:6]1[C:5]2[C:4](=[CH:3][C:2]([Cl:1])=[CH:9][CH:8]=2)[N:10]([C:11]([O:13][CH2:14][CH3:15])=[O:12])[C:17]=1[CH2:18][C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([N+:26]([O-:28])=[O:27])[CH:21]=1

Participants

3

Reactant 2

HCID 752132-Bromo-1-(3-nitrophenyl)ethan-1-oneHCID 183678884-Chloro-2-[(ethoxycarbonyl)amino]benzonitrile

Product 1

HCID 21710899HCID 21710899, compound

Procedure

The title compound was prepared according to the procedure described in step 2 of Example I from 4-chloro-2-[(ethoxycarbonyl)amino]benzonitrile (Example 1, step 1) and 2-bromo-3′-nitroacetophenone.

Sources & evidence

ORD record
ord-14099dc9de744364b60b33f7eef6e5ad
Source dataset
uspto-grants-2001_08
Patent number
US06277878B1

Reaction notes

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