Methanesulfonyl chloride → HCID 9818970, compound

HRID 651032Notes

Reaction equation

[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][C:7]([F:11])=[CH:8][CH:9]=2)[N:4](C(OCC)=O)[C:3]=1[C:17](=[O:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.[CH3:25][S:26](Cl)(=[O:28])=[O:27]>>[C:17]([C:3]1[NH:4][C:5]2[C:10]([C:2]=1[NH:1][S:26]([CH3:25])(=[O:28])=[O:27])=[CH:9][CH:8]=[C:7]([F:11])[CH:6]=2)(=[O:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 18367847HCID 18367847, compound

Product 1

HCID 9818970HCID 9818970, compound

Procedure

The title compound was prepared according to the procedure described in Example 38 from ethyl 3-amino-2-benzoyl-6-fluoro-1H-indole-1-carboxylate (step 2) and methanesulfonyl chloride.

Sources & evidence

ORD record: ord-e123014beca540229f1f28c20484667e
Source dataset: uspto-grants-2001_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06277878B1

Reaction notes

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