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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 651122Generated: October 29, 2026

1,4-Dioxane hydrochloride → HCID 21710727, compound

https://huagongshe.com/reaction/651122

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,4-Dioxane hydrochlorideHCID 20443148—
ReactantHCID 53784664HCID 53784664—
ProductHCID 21710727HCID 21710727—

Reaction Conditions

Temperature25 °C

Reaction Steps

(2-Oxo-2-thiazolidin-3-yl-ethyl)-carbamic acid tert-butyl ester (5.41 g, 22 mmol) was dissolved in 4M HCl-dioxane (80 mL) at 0° C. The resulting solution was stirred at 25° C. for 2 hours, concentrated and the residue triturated with ether. Yield, 3.9 g, 97%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06277877B1
Source datasetuspto-grants-2001_08
ORD IDord-2dc5e273c01a477681ff7c1952295c4a
Source noteuspto-grants-2001_08