HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-D-phenylalanine → HCID 7201349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-D-phenylalanine | HCID 637610 | — |
| Reactant | Methylamine hydrochloride | HCID 6364545 | — |
| Product | HCID 7201349 | HCID 7201349 | — |
Reaction Steps
Methylamine hydrochloride (3.1 mmol) and Boc-D-phenyl-alanine (2.8 mmol) were coupled according to Procedure A (0-25° C. reaction temperature, 144 hour reaction time, washed with acid first, then base) giving the product which was used without further purification. Yield 760 mg, 96%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277877B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-209299cac4134787b06604dd6306d8b0 |
| Source note | uspto-grants-2001_08 |