HuagongsheHuagongshe Chemistry Print Report · For research reference only
((1S)-1-Methylcarbamoyl-2-phenyl-ethyl)-carbamic acid tert-butyl ester → HCID 13689669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ((1S)-1-Methylcarbamoyl-2-phenyl-ethyl)-carbamic acid tert-butyl ester | HCID 7201346 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 13689669 | HCID 13689669 | — |
Reaction Steps
[((1S)-1-Methylcarbamoyl-2-phenyl-ethyl)-carbamic acid tert-butyl ester (2.35 g, 8.45 mmol) was dissolved in 4 M HCl-dioxane (20 ml) at 25° C. for 2 hours. The mixture was concentrated and the residue triturated with ether, and dried. Yield 1.70 g, 94%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06277877B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-5711be03a56f432985d3a62eb8c8e864 |
| Source note | uspto-grants-2001_08 |