HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 651192Generated: October 30, 2026
1,4-Dioxane hydrochloride → HCID 69688374, compound
https://huagongshe.com/reaction/651192
Participants
| Role | Name | HCID | Charge |
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| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 69688105 | HCID 69688105 | — |
| Product | HCID 69688374 | HCID 69688374 | — |
Reaction Steps
[(1S)-Benzyl-2-(1,3-dihydro-isoindol-2-yl)-2-oxo-ethyl]-carbamic acid tert-butyl ester (88 mg) was dissolved in cold 4N HCl-dioxane (1.5 mL), stirred 2 h at 25° C., and the mixture concentrated. The residue was triturated with ether and dried (65 mg, 91%). TSPMS 267 (MH+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06277877B1 |
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| Source dataset | uspto-grants-2001_08 |
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| ORD ID | ord-194a65b9644e46a8adef7c930a136940 |
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| Source note | uspto-grants-2001_08 |
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