Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Methylacetanilide | HCID 12107 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22465461 | HCID 22465461 | — |
Reaction Steps
N-phenylpropionamide(7.46 g, 0.05 mol) and pyridine(13.8 g, 0.18 mol) were dissolved in dichloromethane(300 g) , and the mixture was cooled to 0° C. And then phosphorus oxychloride(8.43 g, 0.05 mol) was added dropwise thereto for 2 hours, and then the mixture was stirred at room temperature (20° C.) for 2 hours to produce N-phenylpropionimidoylchloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06277995B1 |
|---|
| Source dataset | uspto-grants-2001_08 |
|---|
| ORD ID | ord-a450742ec61840b48fca982ca1cdeb84 |
|---|
| Source note | uspto-grants-2001_08 |
|---|
