HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 178426088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | 6-chloro-4-methyl-1,3-benzothiazole-2-thiol | HCID 178426089 | — |
| Product | HCID 178426088 | HCID 178426088 | — |
Reaction Steps
8.6 g of 6-chloro-2-mercapto-4-methylbenzothiazole are reacted with 4.4 g of maleic anhydride in 70% H2SO4 at 47°-50° as described in Example 1. The crude product is purified by reprecipitation from NaHCO3 solution. 6-Chloro-4-methylbenzothiazol-2-ylthiosuccinic acid of melting point 168°-171°, with decomposition, is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04612378 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-7ff7b6648935401dbd81172b0811649f |
| Source note | uspto-grants-1986_09 |