HRID65135

反应详情

EQUATION

反应方程式

HRID 65135 的结构方程式

CONDITIONS

反应条件

温度
170 °C

PROCEDURE

实验过程

The following example illustrates the use of basic amine catalysts. A mixture of benzoyl chloride (7.03 g, 0.05 mole), diallyl carbonate (7.10 g, 0.05 mole) and N,N-dimethylaminopyridine (0.06 g) were combined in a glass reaction vessel and heated to 170° C. for 4 hours. Distillation of the reaction mixture gave allyl benzoate, b.p. 110° C.-111° C. (13 mm Hg). Yield was 90 percent.

WORKUP

后处理

  1. customwere combined in a glass reaction vessel
  2. distillationDistillation of the reaction mixture