HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54463660, compound → HCID 10656658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54463660 | HCID 54463660 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10656658 | HCID 10656658 | — |
Reaction Steps
A solution of ethyl (1-azabicyclo[3.2.1]octan-6-ylidene)cyanoacetate (41 g, 0.19 mol) in abs. ethanol (500 ml) was treated with 10% palladium on carbon (5 g) and hydrogen in a Parr shaker at 30 psi for 5 h. Filtration and evaporation gave the title compound in 36 g yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06281232B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-3e852ec5778e40819ea35923b929ce76 |
| Source note | uspto-grants-2001_08 |