HCID 86757272, compound → HCID 70236857, compound

Participants

Reaction Steps

0.6 g of 10% Pd/C is added to a solution of 7 mmol of the compound obtained in Step 1 in 160 ml of ethyl acetate. The reaction mixture is then stirred under hydrogen for 16 hours and subsequently filtered over Celite. After concentration of the fil trate under reduced pressure, the residue is chromatographed on silica gel (dichloromethane/ethyl acetate: 90/10), enabling the expected product to be isolated.

Provenance & Evidence