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HRID651609

反应详情

EQUATION

反应方程式

HRID 651609 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N[C@H]1CCNC1=O
HCID10750535

tert-Butyl [(3S)-2-oxopyrrolidin-3-yl]carbamate

C9H16N2O3

结构：Clc1ccc2ccc(CBr)cc2n1
HCID11334357

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N[C@H]1CCN(Cc2ccc3ccc(Cl)nc3c2)C1=O
HCID54270233

未命名化合物

PROCEDURE

实验过程

The title compound is prepared from (2-oxopyrrolidin-3-(S)-yl)-carbamic acid tert-butyl ester as described in EXAMPLE 1, Part H using 7-bromomethyl-2-chloro-quinoline in place of 7-bromomethyl-1-chloro-isoquinoline. The crude product is triturated in 20% EtOAc/hexanes and filtered to afford the title compound as a beige solid.

WORKUP

后处理

  1. customThe crude product is triturated in 20% EtOAc/hexanes
  2. filtrationfiltered