HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chlorobenzo[b]thiophene-2-sulfonyl chloride → HCID 54485528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chlorobenzo[b]thiophene-2-sulfonyl chloride | HCID 15158641 | — |
| Reactant | HCID 70023315 | HCID 70023315 | — |
| Product | HCID 54485528 | HCID 54485528 | — |
Reaction Steps
The title compound is prepared as described in EXAMPLE 1, Part K using 6-chloro-benzo[b]thiophene-2-sulfonyl chloride and 2-(3-(S)-amino-2-oxopyrrolidin-1-ylmethyl)-pyrrolo[3,2-b]pyridine-1-carboxylic acid ethyl ester hydrochloride as starting material. The crude product is purified by column chromatography eluting with 60% EtOAc/CH2Cl2 to provide the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06281227B1 |
| Source dataset | uspto-grants-2001_08 |
| ORD ID | ord-2ff8b356a0fc4d38bee4b81addc69518 |
| Source note | uspto-grants-2001_08 |