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HRID651667

反应详情

EQUATION

反应方程式

HRID 651667 的结构方程式

REACTANTS

反应物

2
结构：O=C(N[C@H]1CCNC1=O)OCc1ccccc1
HCID11447643

Benzyl [(3S)-2-oxopyrrolidin-3-yl]carbamate

C12H14N2O3

结构：BrCc1ccc2ccnc(Oc3ccccc3)c2c1
HCID18176415

未命名化合物

PRODUCTS

生成物

1
结构：O=C(N[C@H]1CCN(Cc2ccc3ccnc(Oc4ccccc4)c3c2)C1=O)OCc1ccccc1
HCID54477422

未命名化合物

PROCEDURE

实验过程

The title compound is prepared as described in Example 1, Part H using 7-bromomethyl-1-phenoxyisoquinoline and [2-oxopyrrolidin-3-(S)-yl]carbamic acid benzyl ester as the starting materials. The crude product is purified by column chromatography eluting with 70% EtOAc/hexanes to afford the title product as a clear oil.

WORKUP

后处理

  1. customThe title compound is prepared
  2. customThe crude product is purified by column chromatography
  3. washeluting with 70% EtOAc/hexanes