N-Methyl-tert-butylamine → HCID 21709104, compound

HRID 651710Notes

Reaction equation

HRID 651710 reaction equation
[C:1]([NH:5][CH3:6])([CH3:4])([CH3:3])[CH3:2].Cl[S:8]([CH2:11][C:12]([O:14][CH3:15])=[O:13])(=[O:10])=[O:9]>>[CH3:15][O:14][C:12](=[O:13])[CH2:11][S:8](=[O:10])(=[O:9])[N:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH3:6]

Participants

3

Reactant 2

HCID 84552N-Methyl-tert-butylamineHCID 11435213Methyl (chlorosulfonyl)acetate

Product 1

HCID 21709104HCID 21709104, compoundYield 60,296.699%

Procedure

The subtitle compound (14.81 g, 59%) was prepared as a yellow oil from tert-butylmethylamine (24.48 g, 0.28 mol) and methyl chlorosulfonylacetate (19.37 g, 0.11 mmol), using the method of Example 1(a).

Sources & evidence

ORD record
ord-787dc1b3c3054eb3b0e7b215b4e0971d
Source dataset
uspto-grants-2001_08
Patent number
US06281357B1

Reaction notes

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