HRID651750

反应详情

EQUATION

反应方程式

REACTANTS

反应物

反应SMILES：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1nccn1C

HCID2763252

1-Methyl-2-(tributylstannyl)-1H-imidazole

C16H32N2Sn

反应SMILES：Cn1cc(C2=C(c3cn(C)c4cc(Br)ccc34)C(=O)NC2=O)c2ccccc21

HCID21709059

未命名化合物

PRODUCTS

产物

反应SMILES：Cn1ccnc1-c1ccc2c(C3=C(c4cn(C)c5ccccc45)C(=O)NC3=O)cn(C)c2c1

HCID10203314

未命名化合物

收率 38%

PROCEDURE

实验过程

3-(1-Methyl-1H-indol-3-yl)-4-[1-methyl-6-(1-methyl-1H-imidazol-2-yl)-1H-indol-3-yl]-pyrrole-2,5-dione (46 mg, 38%) was prepared from 3-(6-bromo-1-methyl-1H-indol-3-yl)-4-(1-methyl-1H-indol-3-yl)pyrrole-2,5-dione (120 mg, 0.28 mmol) and 1-methyl-2-(tributylstannyl)imidazole (0.8 mL, containing 50% 1-methyl-imidazole) (Molloy, K. C.; Waterfield, P. C.; Mahon, M. F. J. Organonetallic. Chem. 1989, 365, 61.)