HCID 57214054, compound → HCID 70452679, compound

HRID 65184Notes

Reaction equation

HRID 65184 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:15][C:8]([CH2:9][S:10][CH2:11][CH2:12]SC)=[CH:7][CH:6]=1)[CH3:3].[N+:16]([CH:19]=[C:20]([NH2:30])[NH:21][CH:22]1[CH2:27][CH2:26][CH2:25][CH2:24][N:23]1[CH2:28][CH3:29])([O-:18])=[O:17]>>[CH3:1][N:2]([CH2:4][C:5]1[O:15][C:8]([CH2:9][S:10][CH2:11][CH2:12][NH:30][C:20]([NH:21][CH:22]2[CH2:27][CH2:26][CH2:25][CH2:24][N:23]2[CH2:28][CH3:29])=[CH:19][N+:16]([O-:18])=[O:17])=[CH:7][CH:6]=1)[CH3:3]

Participants

3

Reactant 2

HCID 57214054HCID 57214054, compoundHCID 704525892-nitro-N-(N-ethylpiperidinyl)-1,1-ethenediamine

Product 1

HCID 70452679HCID 70452679, compound

Procedure

24.54 grams of 2-[[5-[(dimethylamino)methyl]furfuryl]thio]ethylmethylsulphide are reacted with 40 grams of 2-nitro-N-(N-ethylpiperidinyl)-1,1-ethenediamine at 80° C. for 3 hours. The mixture is cooled and the procedure described in Example 1 is followed. The product melts at 95°-98° C.; spectrophotometric analyses confirm its structure.

Workup

  1. temperatureThe mixture is cooled

Sources & evidence

ORD record
ord-1a048371f955493a8ca5212ebc9ce2d6
Source dataset
uspto-grants-1986_09
Patent number
US04613596

Reaction notes

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