HCID 57214054, compound → HCID 70452728, compound

HRID 65185Notes

Reaction equation

HRID 65185 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:15][C:8]([CH2:9][S:10][CH2:11][CH2:12]SC)=[CH:7][CH:6]=1)[CH3:3].[N+:16]([CH:19]=[C:20]([NH2:28])[NH:21][CH:22]1[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]1)([O-:18])=[O:17]>>[CH3:1][N:2]([CH2:4][C:5]1[O:15][C:8]([CH2:9][S:10][CH2:11][CH2:12][NH:28][C:20]([NH:21][CH:22]2[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]2)=[CH:19][N+:16]([O-:18])=[O:17])=[CH:7][CH:6]=1)[CH3:3]

Participants

3

Reactant 2

HCID 57214054HCID 57214054, compoundHCID 70452616N~1~-Cyclohexyl-2-nitroethene-1,1-diamine

Product 1

HCID 70452728HCID 70452728, compound

Procedure

24.54 grams of 2-[[5-[(dimethylamino)methyl]furfuryl]thio]ethylmethylsulphide are reacted with 37 grams of 2-nitro-N-cyclohexyl-1,1-ethenediamine at 80° C. for 3 hours. Th mixture is cooled and the procedure described in Example 1 is followed. The product melts at 97°-99° C. Spectrophotometric analyses confirm its structure.

Workup

  1. temperatureTh mixture is cooled

Sources & evidence

ORD record
ord-c3879ca5c43b4b3aaaf9826255f83568
Source dataset
uspto-grants-1986_09
Patent number
US04613596

Reaction notes

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