HCID 57214054, compound → HCID 70452772, compound

HRID 65186Notes

Reaction equation

HRID 65186 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:15][C:8]([CH2:9][S:10][CH2:11][CH2:12]SC)=[CH:7][CH:6]=1)[CH3:3].[N+:16]([CH:19]=[C:20]([NH:22][CH:23]([C:25]1[CH2:30][CH:29]=[CH:28][CH2:27][CH:26]=1)[CH3:24])[NH2:21])([O-:18])=[O:17]>>[CH3:1][N:2]([CH2:4][C:5]1[O:15][C:8]([CH2:9][S:10][CH2:11][CH2:12][NH:21][C:20]([NH:22][CH:23]([C:25]2[CH2:30][CH:29]=[CH:28][CH2:27][CH:26]=2)[CH3:24])=[CH:19][N+:16]([O-:18])=[O:17])=[CH:7][CH:6]=1)[CH3:3]

Participants

3

Reactant 2

HCID 57214054HCID 57214054, compoundHCID 70452623HCID 70452623, compound

Product 1

HCID 70452772HCID 70452772, compound

Procedure

24.54 grams of 2-[[5-[(dimethylamino)methyl]furfuryl]thio]ethylmethylsulphide are reacted with 41 grams of 2-nitro-N'-(1,4-cyclohexadienyl-2-ethyl)-1,1-ethenediamine at 80° C. for 3 hours. The mixture is cooled and the procedure described in Example 1 is followed. Spectrophotometric analyses confirm the structure of the compound obtained.

Workup

  1. temperatureThe mixture is cooled
  2. customobtained

Sources & evidence

ORD record
ord-084baca209bb4e23a232ff4124875409
Source dataset
uspto-grants-1986_09
Patent number
US04613596

Reaction notes

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