HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 2-(4-Acetoxypiperidino)-5-(2,4-dichlorophenyl)pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-(4-Hydroxypiperidino)-5-(2,4-dichlorophenyl)pyrimidine | HCID 13605523 | — |
| Product | 2-(4-Acetoxypiperidino)-5-(2,4-dichlorophenyl)pyrimidine | HCID 20234099 | — |
Reaction Steps
6 g of 2-(4-hydroxypiperidino)-5-(2,4-dichlorophenyl)pyrimidine (Example 5) and 60 ml of acetic anhydride are heated under reflux for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04613603 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-2f74be5623254999b46f8ab2f9d21007 |
| Source note | uspto-grants-1986_09 |