HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → HCID 20198240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | Glycol monoethyl ether | HCID 8076 | — |
| Reactant | 4-[14-(Trimethylsilyl)tetradecylamino)benzoic acid | HCID 13884862 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20198240 | HCID 20198240 | — |
Reaction Steps
A solution of 11.5 g. of 4-[14-(trimethylsilyl)tetradecylamino]benzoic acid, 1.00 g. of 2-ethoxyethanol and 5.35 ml. of boron trifluoride etherate in 200 ml. of toluene is stirred at reflux for 48 hours. The solution is treated with an additional 5.35 ml. of boron trifluoride etherate and refluxing is continued for 120 hours. Dilution with water and methylene chloride followed by filtration affords the product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670421 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-84da5973c2b245439a03fec1f72da3db |
| Source note | uspto-grants-1987_06 |