HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lactic Acid → HCID 20198274, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lactic Acid | HCID 612 | — |
| Reactant | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| Reactant | 4-[14-(Trimethylsilyl)tetradecylamino)benzoic acid | HCID 13884862 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20198274 | HCID 20198274 | — |
Reaction Steps
A flask containing 10.0 g. 4-[14-(trimethylsilyl)tetradecylamino]benzoic acid, 3.4 g. lactic acid, 500 mg. toluenesulfonic acid and 500 ml. toluene is equipped with a Soxhlet extractor charged with activated 4A Linde molecular sieves. The solution is refluxed for 24 hours, during which time the Soxhlet extractor is charged twice more with fresh sieves. The hot solution is filtered and allowed to cool, whereupon the product separates as off-white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670421 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-fc34777c7db64b5c8b6e080d1deff3be |
| Source note | uspto-grants-1987_06 |