HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 13911284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 3-[2-[4-(2-Methoxyphenyl)piperazin-1-yl]ethyl]thieno[3,2-d]pyrimidine-2,4-dione | HCID 13911278 | — |
| Product | HCID 13911284 | HCID 13911284 | 61% |
Reaction Steps
The title compound was produced following the procedure of Example 13 using dimethylformamide as the solvent and the thienopyrimidine-2,4-dione (1.82 g, 4.66 mmol) from Example 19. The title compound was isolated in 61% yield (1.13 g) after recrystallization from EtOH, mp 149°-151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04670560 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-2821f43c18434f149fdb23e6c0e9d1d2 |
| Source note | uspto-grants-1987_06 |