HCID 13957226, compound → HCID 18608218, compound

HRID 652467Notes

Reaction equation

[P:1]([O:5][CH2:6][C@H:7]1[O:11][C@@H:10]([N:12]2[CH:19]=[C:18]([NH2:20])[C:16](=[O:17])[NH:15][C:13]2=[O:14])[CH2:9][C@@H:8]1[OH:21])([OH:4])([OH:3])=[O:2].[N:22]([O-])=O.[Na+]>>[P:1]([O:5][CH2:6][C@H:7]1[O:11][C@@H:10]([N:12]2[CH2:19][C:18](=[N+:20]=[N-:22])[C:16](=[O:17])[NH:15][C:13]2=[O:14])[CH2:9][C@@H:8]1[OH:21])([OH:3])([OH:4])=[O:2]

Participants

Reactant 2

HCID 13957226HCID 13957226, compound

HCID 23668193Sodium Nitrite

Product 1

HCID 18608218HCID 18608218, compound

Procedure

acidifying said 5-amino-2'-deoxyuridine-5'-monophosphate and reacting the acidified product with sodium nitrite to produce 5-diazo-2'-deoxyuridine-5'-monophosphate;

Sources & evidence

ORD record: ord-fa8439e764cc407890050e7e101ce8b2
Source dataset: uspto-grants-1987_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04672111

Reaction notes

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