HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine, 3-(4-aminobutyl)- → 7(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyl)butyl]heptanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine, 3-(4-aminobutyl)- | HCID 72927 | — |
| Reactant | 7-(4-Acetyl-3-hydroxy-2-propylphenoxy)heptanoic acid | HCID 13753883 | — |
| Product | 7(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyl)butyl]heptanamide | HCID 13912785 | — |
Reaction Steps
7-(4-Acetyl-3-hydroxy-2-propylphenoxy)heptanoic acid was allowed to react with 3-pyridine butanamine according to procedure A and the product was purified by chromatography on silica gel to give 7(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyl)butyl]heptanamide, the title compound, mp 57°-59° (from acetone-hexane) in 75% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672066 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-dd8a7072585d455ba474aac402057fe7 |
| Source note | uspto-grants-1987_06 |