HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine, 3-(4-aminobutyl)- → 4-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyl)butyl]butanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine, 3-(4-aminobutyl)- | HCID 72927 | — |
| Reactant | 4-(4-Acetyl-3-hydroxy-2-propylphenoxy)butanoic acid | HCID 13753871 | — |
| Product | 4-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyl)butyl]butanamide | HCID 13912780 | — |
Reaction Steps
4-(4-Acetyl-3-hydroxy-2-propylphenoxy)butanoic acid was allowed to react with 3-pyridine butanamine according to procedure A and the product was purified by HPLC to give 4-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyl)butyl]butanamide, the title compound, mp 80°-82° (from ether) in 68% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672066 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-8789b40e71a842c2be68b3132b6082c5 |
| Source note | uspto-grants-1987_06 |