huagongshe.com
HRID652478

反应详情

EQUATION

反应方程式

HRID 652478 的结构方程式

REACTANTS

反应物

2
结构：NCCCCc1cccnc1
HCID72927

Pyridine, 3-(4-aminobutyl)-

C9H14N2

结构：CCCc1c(OCC(=O)O)ccc(C(C)=O)c1O
HCID13753869

(4-Acetyl-3-hydroxy-2-propylphenoxy)acetic acid

C13H16O5

PRODUCTS

生成物

1
结构：CCCc1c(OCC(=O)NCCCCc2cccnc2)ccc(C(C)=O)c1O
HCID13912786

未命名化合物

PROCEDURE

实验过程

(4-Acetyl-3-hydroxy-2-propylphenoxy)acetic acid was allowed to react with 3-pyridine butanamine according to procedure A and the product was purified by chromatography on silica gel to give (4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyl)butyl]acetamide, the title compound, mp 95°-97° (from methylene chloride-ether) in 57% yield.

WORKUP

后处理

  1. customthe product was purified by chromatography on silica gel