HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Pyridin-3-yl)propan-1-amine → 6-(4-Acetyl-3-hydroxy-2-propylphenoxy)-N-[3-(3-pyridinyl)propyl]hexanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Pyridin-3-yl)propan-1-amine | HCID 13557523 | — |
| Reactant | 6-(4-Acetyl-3-hydroxy-2-propylphenoxy)hexanoic acid | HCID 13753873 | — |
| Product | 6-(4-Acetyl-3-hydroxy-2-propylphenoxy)-N-[3-(3-pyridinyl)propyl]hexanamide | HCID 13912773 | — |
Reaction Steps
6-(4-Acetyl-3-hydroxy-2-propylphenoxy)hexanoic acid was allowed to react with 3-pyridine propanamine according to procedure A and the product was purified by chromatography on silica gel to give 6-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[3-(3-pyridinyl)propyl]hexanamide the title compound, mp 83°14 85° (from methylene chloride-ether) in 87% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672066 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-3daf8d6ff5b041d9b3a91b2fcf7162e9 |
| Source note | uspto-grants-1987_06 |