huagongshe.com
HRID652480

反应详情

EQUATION

反应方程式

HRID 652480 的结构方程式

REACTANTS

反应物

2
结构：NCCCCCCc1cccnc1
HCID13557453

6-(Pyridin-3-yl)hexan-1-amine

C11H18N2

结构：CCCc1c(OCCCC(=O)O)ccc(C(C)=O)c1O
HCID13753871

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1c(OCCCC(=O)NCCCCCCc2cccnc2)ccc(C(C)=O)c1O
HCID13912781

未命名化合物

PROCEDURE

实验过程

4-(4-Acetyl-3-hydroxy-2-propylphenoxy)butanoic acid was allowed to react with 3-pyridine hexanamine according to procedure A and the product was purified by chromatography on silica gel to give 4-(4-acetyl-3-hydroxy- 2-propylphenoxy)-N-[6-(3-pyridinyl)hexyl]butanamide, the title compound, mp 69°-71° (from ether-hexane) in 84% yield.

WORKUP

后处理

  1. customthe product was purified by chromatography on silica gel