HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Pyridin-3-yloxy)butan-1-amine → 6-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyloxy)butyl]hexanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Pyridin-3-yloxy)butan-1-amine | HCID 12112219 | — |
| Reactant | 6-(4-Acetyl-3-hydroxy-2-propylphenoxy)hexanoic acid | HCID 13753873 | — |
| Product | 6-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyloxy)butyl]hexanamide | HCID 13912778 | — |
Reaction Steps
6-(4-Acetyl-3-hydroxy-2-propylphenoxy)hexanoic acid was allowed to react with 4-(3-pyridinyloxy)butyl amine according to procedure A and the product was purified by HPLC to give 6-(4-acetyl-3-hydroxy-2-propylphenoxy)-N-[4-(3-pyridinyloxy)butyl]hexanamide, the title compound, mp 50°-53° (from ethyl acetate) in 73% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672066 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-4044506a43b04c5abf2e33fbfd2a1109 |
| Source note | uspto-grants-1987_06 |