HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine, 3-(4-aminobutyl)- → HCID 20197288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine, 3-(4-aminobutyl)- | HCID 72927 | — |
| Reactant | HCID 13912821 | HCID 13912821 | — |
| Reactant | HCID 86741580 | HCID 86741580 | — |
| Product | HCID 20197288 | HCID 20197288 | 73% |
Reaction Steps
3-[(4-Acetyl-3-hydroxy-2-propylphenoxy)methyl]-2-ethoxybenzoic acid was allowed to react with 3-pyridine butanamine according to the procedure of Example 32 and the product was purified by recrystallization from methylene chloride-ether to give, 3-[(4-Acetyl-3-hydroxy-2-propylphenoxy-methyl]-2-ethoxy-[4-(3-pyridinyl)butyl]benzamide, the title compound, mp 107°-109° in 73% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672066 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-5056da086ddc44d1812a1297ce107d9e |
| Source note | uspto-grants-1987_06 |