HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Benzyloxyphenyl)ethylacetoacetate → 2-(4-Hydroxyphenyl)ethylacetoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Benzyloxyphenyl)ethylacetoacetate | HCID 13632568 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(4-Hydroxyphenyl)ethylacetoacetate | HCID 131715181 | 97.5% |
Reaction Steps
A solution of 6.2 g of 2-(4-benzyloxyphenyl)ethylacetoacetate in 100 mL of ethanol with 0.5 g of 10% palladium on carbon was hydrogenated at 50 psi for 18 h. The mixture was filtered and the filtrate evaporated to afford 4.3 g of 2-(4-hydroxyphenyl)ethylacetoacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672071 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-eac97179f94a432aa10d4734d2ad58b0 |
| Source note | uspto-grants-1987_06 |