HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → 5-(p-Methoxybenzylidene)-hydantoin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | Glycine | HCID 750 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | Disodium glutamate | HCID 167560 | — |
| Product | 5-(p-Methoxybenzylidene)-hydantoin | HCID 94749 | — |
Reaction Steps
5-(p-Methoxybenzylidene)-hydantoin was prepared in the same manner as in Example 4, except that 46.8 g (0.25 mol) of sodium L-glutamate.monohydrate and 68.1 g (0.50 mol) of p-methoxybenzaldehyde were used in lieu of glycine and p-hydroxybenzaldehyde, respectively. During the reaction, the pH of the reaction mixture was 9.9 to 9.7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04672127 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-21a593b0f39944088baeaee864758153 |
| Source note | uspto-grants-1987_06 |