HCID 10986642, compound → HCID 15595109, compound

HRID 652607Notes

Reaction equation

HRID 652607 reaction equation
[Cl:1][C:2]1[CH:37]=[C:36]([C:38]([F:41])([F:40])[F:39])[CH:35]=[CH:34][C:3]=1[O:4][C:5]1[CH:10]=[CH:9][C:8]([N:11](SN(CCC)CCC)[C:12]([NH:14][C:15](=[O:24])[C:16]2[C:21]([F:22])=[CH:20][CH:19]=[CH:18][C:17]=2[F:23])=[O:13])=[C:7]([F:33])[CH:6]=1.[CH:42]([N:45]([CH:48]([CH3:50])[CH3:49])[S:46]Cl)([CH3:44])[CH3:43]>>[Cl:1][C:2]1[CH:37]=[C:36]([C:38]([F:41])([F:39])[F:40])[CH:35]=[CH:34][C:3]=1[O:4][C:5]1[CH:10]=[CH:9][C:8]([N:11]([S:46][N:45]([CH:48]([CH3:50])[CH3:49])[CH:42]([CH3:44])[CH3:43])[C:12]([NH:14][C:15](=[O:24])[C:16]2[C:21]([F:22])=[CH:20][CH:19]=[CH:18][C:17]=2[F:23])=[O:13])=[C:7]([F:33])[CH:6]=1

Participants

3

Reactant 2

HCID 10986642HCID 10986642, compoundHCID 15595108HCID 15595108, compound

Product 1

HCID 15595109HCID 15595109, compound

Procedure

39 was prepared, as a white solid, m.p.: 147°-149° C. in a similar manner to (38). The intermediate compound, di(isopropyl)aminosulphenyl chloride, boiled at 92°-4° C. at 20 Torr.

Sources & evidence

ORD record
ord-607ecccd8fb54c49975928f61da1076f
Source dataset
uspto-grants-1987_06
Patent number
US04672139

Reaction notes

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