HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → Benzyl Benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Decane | HCID 15600 | — |
| Product | Benzyl Benzoate | HCID 2345 | 89% |
Reaction Steps
Two grams of sodium-supported hydrotalcite prepared in Example 7, (1) and stabilized in Example 7 (2) was put in a container holding 20 g of dehydrated benzaldehyde and 35 g of n-decane as a solvent, and reacted at room temperature for 3 hours. The product was analyzed by gas chromatography (OV-17, 2 m). The conversion of benzaldehyde was 90%, and benzyl benzoate was obtained in a yield of 89%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04675307 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-b9aede0675de4cfe886dc91ecea00730 |
| Source note | uspto-grants-1987_06 |