HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-3-buten-1-ol → 3-Methyl-3-butenyl 2-methylisocrotonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-3-buten-1-ol | HCID 12988 | — |
| Reactant | Methyl (2Z)-2-methyl-2-butenoate | HCID 5356352 | — |
| Reactant | Dioctyltin laurate | HCID 22292224 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3-Methyl-3-butenyl 2-methylisocrotonate | HCID 16205381 | — |
Reaction Steps
A mixture of 20.0 g. of methyl angelate, 22.65 g. of 3-methyl-3-butenyl alcohol, 100 ml. of toluene and 0.8 g. of dioctyltin laurate was reacted under the same conditions as in Example 6. The reaction mixture was subjected to single distillation to obtain 39.5 g. of a distillate boiling at 104° C. (32 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04613680 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-af7ccfea57244031a639864f8090c451 |
| Source note | uspto-grants-1986_09 |