HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hexenol → 2-Butenoic acid, 2-methyl-, (3Z)-3-hexenyl ester, (2Z)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hexenol | HCID 5281167 | — |
| Reactant | Methyl (2Z)-2-methyl-2-butenoate | HCID 5356352 | — |
| Reactant | Dioctyltin laurate | HCID 22292224 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-Butenoic acid, 2-methyl-, (3Z)-3-hexenyl ester, (2Z)- | HCID 16220109 | — |
Reaction Steps
A mixture of 20.0 g. of methyl angelate, 26.34 g. of (Z)-3-hexenyl alcohol, 100 ml. of toluene and 1.2 g. of dioctyltin laurate was placed in a 300 ml. glass flask, which was equipped with a Soxhlet extractor filled on the top with molecular sieve 4A and a reflux cooler.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04613680 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-86d99ad2c96d423794886a4f3cc76510 |
| Source note | uspto-grants-1986_09 |