Water → HCID 19850731, compound

HRID 653220Notes

Reaction equation

HRID 653220 reaction equation
[P:1]([O-:8])([O:5]CC)[O:2]CC.O.[CH2:10]([O:19][CH2:20][CH2:21][CH2:22][NH2:23])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH:16]([CH3:18])[CH3:17]>C(O)C>[CH2:10]([P:1](=[O:2])([O-:5])[O-:8])[CH3:11].[CH2:10]([O:19][CH2:20][CH2:21][CH2:22][NH3+:23])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH:16]([CH3:17])[CH3:18].[CH2:10]([O:19][CH2:20][CH2:21][CH2:22][NH3+:23])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH:16]([CH3:17])[CH3:18]

Participants

5

Reactant 3

HCID 962WaterHCID 1218101-Propanamine, 3-(isononyloxy)-HCID 3780918Diethylphosphite

Product 1

HCID 19850731HCID 19850731, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

A mixture of 13.81 g. (0.1 moles) of diethyl phosphite, 20 ml. of water and 20 ml. of ethanol is reacted with a mixture of 20.13 g. (0.1 moles) of 3-isononyloxypropyl amine and 30 ml. of ethanol as described in Example 1. nD30 =1.4485 (liquid fraction).

Workup

  1. additionA mixture of 13.81 g

Sources & evidence

ORD record
ord-49eeb95697904b7782a054617e4b81ee
Source dataset
uspto-grants-1987_06
Patent number
US04675431

Reaction notes

Loading…