HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Dihydroxyanthraquinone → 1,8,10-Trihydroxy-10-phenyl-9-anthrone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Dihydroxyanthraquinone | HCID 2950 | — |
| Reactant | HCID 178506676 | HCID 178506676 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1,8,10-Trihydroxy-10-phenyl-9-anthrone | HCID 12385845 | — |
Reaction Steps
The process of the present invention comprises reacting phenyl lithium with 1,8-dihydroxy anthraquinone in the presence of an anhydrous organic solvent, such as tetrahydrofuran, to form 1,8,10-trihydroxy-10-phenyl-9-anthrone which is then reduced with a reducing agent so as to produce 1,8-dihydroxy-10-phenyl-9-anthrone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04677123 |
| Source dataset | uspto-grants-1987_06 |
| ORD ID | ord-80e3bf9330cf4c7da808df55d2482d9a |
| Source note | uspto-grants-1987_06 |