HRID653498

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCCCCN1C(=O)C2CC(c3ccc([N+](=O)[O-])cc3)(C2)C1=O

HCID14872631

未命名化合物

PRODUCTS

生成物

结构：CCCCCN1C(=O)C2CC(c3ccc(N)cc3)(C2)C1=O

HCID14872636

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23938

Palladium

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

In a manner analogous to that described in Example 1, 2.58 g of 1-(4-nitrophenyl)-3-n-pentyl-3-azabicyclo[3.1.1]heptane-2,4-dione in 75 ml of ethanol are hydrogenated in the presence of 0.15 g of palladium-on-carbon and worked up. Melting point 92°-94° (from ethyl acetate/petroleum ether).