HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Methoxyphenyl)phenol → (S)-3'-(2-Methyloctanoyloxy)-4-methoxy-1,1'-biphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Methoxyphenyl)phenol | HCID 10285870 | — |
| Reactant | (S)-2-methyloctanoylchloride | HCID 53713863 | — |
| Product | (S)-3'-(2-Methyloctanoyloxy)-4-methoxy-1,1'-biphenyl | HCID 53720688 | — |
Reaction Steps
Using 3'-hydroxy-4-methoxy-1,1'-biphenyl (4.2 g, 20.4 mmol) obtained in Example 1, (3) and (S)-2-methyloctanoylchloride (4.1 g, 21.5 mmol), the reaction was carried out in the same manner as described in Example 1, (5), to give the title compound as a pale yellow oil; yield: 5.4 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05128062 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-dd9754bbb34549c781b6f6976e72ce58 |
| Source note | uspto-grants-1992_07 |