HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-hydroxybenzoic acid → (R)-3-chloro-4-(2-n-hexyloxypropanoyloxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-hydroxybenzoic acid | HCID 19860 | — |
| Reactant | (R)-2-n-hexyloxypropanoyl chloride | HCID 22844813 | — |
| Product | (R)-3-chloro-4-(2-n-hexyloxypropanoyloxy)benzoic acid | HCID 22844815 | — |
Reaction Steps
Using 3-chloro-4-hydroxybenzoic acid 1/2 hydrate (3.76 g, 20.7 mmol) and (R)-2-n-hexyloxypropanoyl chloride (3.98 g, 20.7 mmol), the reaction was carried out in the same manner as described in Example 4, (1), to give the title compound as a pale yellow oil; yield: 2.60 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05128062 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-4044d592bc5244ebbebd20288d3639ca |
| Source note | uspto-grants-1992_07 |