Acetic Acid → HCID 12998343, compound

HRID 653605Notes

Reaction equation

HRID 653605 reaction equation
[CH2:1]([NH:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].[C:10]([OH:13])(=[O:12])[CH3:11]>>[C:10]([OH:13])(=[O:12])[CH3:11].[CH2:1]([NH:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 176Acetic AcidHCID 8148Dibutylamine

Product 1

HCID 12998343HCID 12998343, compound

Procedure

Into a twelve liter Morton flask equipped with stirrer, thermometer, reflux condenser, heating mantle, and addition funnel are placed 89 grams (0.69 moles) of di-n-butyl amine and 42 grams (0.69 moles) of acetic acid. The resulting reaction mass temperature rises to 50° C. (as a result of salt formation to form di-n-butyl amine acetate). The reaction mass is cooled to 38° C. and rapidly, 1600 grams (19.74 moles) of 37% formaldehyde (effective weight 592 grams) is added to the reaction mass.

Workup

  1. customInto a twelve liter Morton flask equipped with stirrer
  2. temperaturethermometer, reflux condenser
  3. temperatureheating mantle
  4. additionaddition funnel
  5. customThe resulting reaction mass temperature
  6. customrises to 50° C.
  7. customa result of salt formation

Sources & evidence

ORD record
ord-aafc052f001043c482278db46599f072
Source dataset
uspto-grants-1992_07
Patent number
US05128317

Reaction notes

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