Dicyclohexylcarbodiimide → HCID 178455950, compound

Participants

Reaction Steps

In a manner analogous to that described in Example 1, using as starting materials 162 mg of Z-Phe-His-OH, 128 mg of H-Leu-Val-Ile-2-(2-pyridyl)-ethyl amide, 57 mg of HOBt and 88 mg of DCCI, the title compound is obtained after flash chromatography (65 g of silica gel 60, 40-63 μm, eluant system B7). Rf (B7)=0.30, Rf (B11)=0.62.

Provenance & Evidence