Ethyl formate → HCID 15029813, compound

Participants

Reaction Steps

The product from Example 14 was converted to its free base (3.4 g) and dissolved into toluene (30 ml). Ethyl formate (5 ml) was added and the reaction stirred at reflux for 5 hr. The solvent was removed to afford a solid. Recrystallization from Et2O/CH2Cl2 afforded 3.07 g of desired product. Anal. calcd. for C13H17NO2 ; C, 71.21; H, 7.81; N, 6.39. Found: C, 71.26; H, 7.82; N, 6.41.

Provenance & Evidence